o-Nitrobenzoyl Chloride Oxime - Names and Identifiers
o-Nitrobenzoyl Chloride Oxime - Physico-chemical Properties
Molecular Formula | C7H5ClN2O3
|
Molar Mass | 200.58 |
Storage Condition | Room Temprature |
o-Nitrobenzoyl Chloride Oxime - Upstream Downstream Industry
o-Nitrobenzoyl Chloride Oxime - Introduction
ALPHA-CHLORO-2-NITROBENZALDOXIME(ALPHA-CHLORO-2-NITROBENZALDOXIME) is an organic compound whose structure contains an ortho chlorine atom, a nitro group and a hydroxoxime group.
Nature:
-Appearance: White crystalline solid
-Melting point: about 125-128°C
-Thermal stability: relatively stable, can be stored and operated under moderate temperature conditions
-Solubility: Soluble in organic solvents (such as ethanol, ether, dichloromethane), insoluble in water
Use:
ALPHA-CHLORO-2-NITROBENZALDOXIME are mainly used in various reactions in organic synthesis and are often used as catalysts or intermediates. It can participate in nucleophilic electrophilic substitution reactions, coupling reactions and other reaction processes. In addition, it also has certain antioxidant properties.
Preparation Method:
ALPHA-CHLORO-2-NITROBENZALDOXIME is prepared by various methods. A common synthetic route is to prepare it by nitrogen hydrogenation and chlorination of substituted benzaldehyde. The specific preparation steps are as follows:
1. take a specific proportion of o-nitrobenzaldehyde and ammonia.
2. Ferrous chloride is added as a catalyst, and the reaction mixture is heated to an appropriate temperature (usually under reflux conditions).
3. After the reaction is completed, cool and wash the product with a suitable organic solvent to remove impurities.
4. Crystallization and purification gave the ALPHA-CHLORO-2-NITROBENZALDOXIME product.
Safety Information:
The ALPHA-CHLORO-2-NITROBENZALDOXIME is relatively stable under general operating conditions, but it is still necessary to pay attention to safe operation measures. Here are some safety considerations:
-Contact: Avoid direct contact with eyes, skin and clothing. If contact occurs, rinse immediately with plenty of water. If discomfort occurs, seek medical attention as soon as possible.
-Inhalation: Avoid inhaling its dust and ensure that the operating area is well ventilated.
-Swallowing: Do not ingest. If accidentally swallowed, seek medical attention immediately.
-Storage: Fully sealed and stored in a cool, dry place, away from flammables and oxidants.
When using ALPHA-CHLORO-2-NITROBENZALDOXIME, follow appropriate laboratory practices and personal protective measures. It is strongly recommended to use this compound after knowledge of relevant safety information and training.
Last Update:2024-04-09 20:52:54